MaTestLab > Test Standards > ASTM E3047 Analysis of Nickel Alloys by Spark Atomic Emission Spectrometry
ASTM E3047 Analysis of Nickel Alloys by Spark Atomic Emission Spectrometry
ASTM E3047 is a standardized test method used for the analysis of nickel alloys using spark atomic emission spectrometry (Spark-AES). This method offers a precise and reliable way to identify and quantify the elemental composition of nickel alloys, ensuring quality control, material characterization, and compliance with industry standards.
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Introduction to ASTM E3047
ASTM E3047 provides a systematic procedure for the analysis of nickel alloys using spark atomic emission spectrometry (Spark-AES), a powerful analytical technique that allows for rapid and simultaneous measurement of multiple elements in metallic materials. Nickel alloys are extensively utilized in various industries, including aerospace, automotive, and oil and gas, where accurate elemental analysis is crucial for product performance and safety.
The analysis of nickel alloys is vital to verify that the alloy composition meets specific requirements, ensuring that the final product possesses the desired mechanical and chemical properties. Elements that are detected in this method are Aluminum, Boron, Carbon, Chromium, Cobalt, Copper, Iron, Magnesium, Manganese, Molybdenum, Niobium, Phosphorus and other elements.
ASTM E3047Test Method
The ASTM E3047 test method employs Spark-AES to determine the elemental composition of nickel alloys. The test is conducted in the following steps:
Spark-AES Analysis
The sample is placed in the Spark-AES instrument, and a high-voltage electrical discharge is applied to create a spark on its surface. This spark excites the atoms in the sample, causing them to emit characteristic light. The emitted light is then analyzed using a spectrometer, which identifies the wavelengths of the emitted light, corresponding to specific elements in the alloy.
Identification of Elements
The emitted light is dispersed and measured to identify the elements present in the alloy and quantify their concentrations.
ASTM E3047Specimens
Specimen details
ASTM E3047 specimen is solid metal, powder, or coating of nickel alloy.
Specimen dimensions
ASTM E3047 does not specify a standard specimen size, as it can vary depending on the form of the nickel alloy being analyzed.
Specimen preparation
Specimens are machine operated, cut, grinded, and polished from materials to ensure a clean and homogenous surface for analysis.
ASTM E3047 Results
The data obtained from the Spark-AES analysis is compared to known spectral patterns of various elements to determine the elemental composition of the nickel alloy. The concentration of each identified element is quantified, providing valuable information for material verification and quality control.
Tests Related to ASTM E3047 ASTM E415 – Standard Test Method for Atomic Emission Vacuum Spectrometric Analysis of Carbon and Low-Alloy Steel is a related standard.
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