ASTM D2116 Standard Specification for FEP Resin Molding and Extrusion Materials

    What is ASTM D2116?

    ASTM D2116 describes a standard specification for molding and extrusion materials based on FEP-fluorocarbon resin. It covers melt-processable fluorinated ethylene propylene (FEP) materials supplied as pellets and excludes recycled FEP materials. ASTM D2116 (Standard Specification for FEP Resin Molding and Extrusion Materials) covers FEP resins made from tetrafluoroethylene and hexafluoropropylene or modified FEP resins containing no more than 2% by weight of other fluoromonomers. Laboratories assess molded specimens for Specific gravity, melting point, tensile strength, elongation, dielectric constant, and dissipation factor. The specification requires the lot’s average test results to meet the applicable requirements. The specification classifies the resins into four types based on their melt flow rate. The standard specifies the requirements for melt flow rate, specific gravity, and melting point, tensile strength, elongation, dielectric constant, and dissipation factor. Laboratories evaluate molded specimens to ensure that the average lot complies with the applicable requirements.

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    Get Certified ASTM D2116 Testing for Reliable FEP Resin Materials

    For successful molding and extrusion processes, FEP resin must have consistent processing, mechanical, thermal and electrical properties. Engineers measure these properties using ASTM D2116 to check lot quality. Testing helps manufacturers classify material performance, track production quality, and confirm that a lot meets standards.

    What is the scope of the ASTM D2116 test standard?

    ASTM D2116 applies to melt-processable FEP molding and extrusion materials. FEP-fluorocarbon resin is a copolymer of tetrafluoroethylene and hexafluoropropylene or a modified FEP-fluorocarbon resin containing not more than 2% by weight of other fluoromonomers. The specification-

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    • Covers FEP resins made from tetrafluoroethylene and hexafluoropropylene with no more than 2% by weight of other fluoromonomers.
    • Describes the different types of FEP resin by melt flow rate.
    • Needs a uniform composition and lack of foreign matter.
    • Evaluates melt flow rate, specific gravity, melting point, tensile strength, elongation, dielectric constant, and dissipation factor.
    • Requires the average lot results to conform to the applicable requirements.

    What are the uses of ASTM D2116 testing?

    ASTM D2116 testing allows manufacturers to assess FEP resin for molding and extruding applications. The specification includes property data for material classification, quality control, and product development.

    This standard:

    • Determines the melt flow rate of FEP resin. 
    • Evaluates specific gravity, melting point, tensile strength, elongation, dielectric constant, and dissipation factor.
    • Helps classify FEP resin into the specified types, lot acceptance, and quality control.
    • Supports selection of FEP resin for molding and extrusion applications.

    Which materials can be tested under ASTM D2116?

    ASTM D2116 covers FEP Resin molding and extrusion materials supplied in pellet form. The covered materials consist of tetrafluoroethylene-hexafluoropropylene copolymers or modified FEP resins containing no more than 2% by weight of other fluoromonomers.

    Why is ASTM D2116 Important?

    ASTM D2116 specifies uniform specifications for FEP resin for molding and extrusion. Manufacturers can use these requirements to control lot quality and verify important processing, mechanical, thermal, and electrical properties.

    ASTM D2116 Equipment and Sample Preparation Guide

    ASTM D2116 allows laboratories to mold FEP resin into test sheets before performing applicable tests. Specimens are compression-molded in a molding press under controlled conditions to ensure uniform thickness. The ASTM D2116 test specification comprises the following procedure-

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    Sample and Specimen DetailsTechnicians assess the FEP resin provided in pellet form.
    Specimen PreparationTechnicians then compress the resin into molded sheets using a picture-frame mold, aluminum foil, and heated steel plates. 
    Specimens Dimension Technicians prepare molded sheets approximately 1.5 ± 0.3 mm thick.
    Instrumentation Melt flow indexer, Compression molding press, Hot mold assembly, Tensile testing machine, Specific-gravity apparatus, Differential scanning calorimeter, Dielectric-property measuring equipment, and Conditioning equipment.

    Testing Procedures and Requirements for ASTM D2116

    ASTM D2116 requires laboratories to test the FEP resin using the applicable procedures for melt flow, molded-specimen properties, and electrical properties. Technicians prepare the molded specimens as per the specified molding procedure and condition specimens as required before testing.

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    Other reference ASTM documents include D150, D618, D638, D792, D883, D1238, D2600, D1708, D3892, D4591, and E691.

    Material Classification and Molded Sheet PreparationTechnicians identify the FEP resin type based on applicable melt flow rate requirements and compression-mold the FEP pellets into sheets with the specified thickness.
    Melt Flow Rate and Specific GravityAnalysts calculate melt flow rate using the applicable extrusion plastometer procedure and specific gravity of the molded specimen using the applicable density method.
    Melting Point and Tensile PropertiesLaboratories determine melting points on differential scanning calorimeters and measure tensile strength and elongation using the applicable tensile test procedure.
    Electrical PropertiesLaboratories determine dielectric constant and dissipation factors at the specified frequencies.
    Result ReportingThe laboratory documents the measured properties and compares the average lot results to the specification requirements.

    ASTM D2116 Testing Process and Data Collection

    Technicians first determine the FEP resin lot and application material type. Then technicians prepare the representative specimens and compression-mold the resin into sheets approximately 1.5 ± 0.3 mm thick. Next, analysts perform the applicable melt flow, specific gravity, melting point, tensile, and electrical-property tests. Then laboratories record the measured values and compare the average lot results with the applicable FEP type requirements. Laboratories measure the following properties: melt flow rate, specific gravity, melting point, tensile strength, elongation, dielectric constant, and dissipation factor.

     This image shows a melt flow indexer used for FEP resin molding and extrusion materials according to ASTM D2116.
    ASTM D2116 Melt Flow Indexer 

    Common Challenges and Troubleshooting

    Reliable and reproducible results require Consistent resin sampling, molding, resin conditioning, and test procedures in compliance with ASTM D2116. Variations in molded-sheet thickness, molding temperature, pressure, or specimen conditioning can affect test results. Common problems include inconsistent resin sampling, incorrect molded-sheet thickness, improper molding temperature, incorrect molding pressure, inadequate specimen conditioning, incorrect tensile specimen preparation, and inaccurate melt flow measurements. Before testing, technicians should confirm the type of resin, molding conditions, specimen size, equipment calibration, and conditioning requirements.

    ASTM D2116 Analysis Results and Interpretation

    • Laboratories report ASTM D2116 data based on the resin type, specimen preparation, testing method, and lot measurement.
    • The specification assesses melt flow rate, specific gravity, melting point, tensile strength, elongation, dielectric constant, and dissipation factor.
    • Laboratories report results for melt flow in g/10 min, melting points in ºC, tensile strength in MPa, dimensions in mm, and elongation in %. 
    • Laboratories compare the lot’s average test results with the applicable requirements for Type I, Type II, Type III, or Type IV FEP resin.

    Link to ASTM D2116

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    FAQ

    Where can I get the astm d2116 tested?
    You can share your astm d2116 testing requirements with MaTestLab. MaTestLab has a vast network of material testing laboratories, spread across the USA and Canada. We support your all material testing needs ranging from specific astm d2116 test to various testing techniques.
    Please contact us for a detailed quote for your astm d2116 testing needs. Cost incurred to carry out different astm d2116 testing methodology depends on the type of raw material; number of samples, coupons, or specimens; test conditions, turn around time etc. Costs of some ASTM testing methods start from $100 and the final value depends upon the factors listed above. Please contact us for the best and latest prices.
    The required number of samples or specimens should comply with the procedure given in the astm d2116 standard. However, the MaTestLab operations team can assist you for your special requirements once you share your testing details with us.
    MaTestLab has a vast testing laboratory network, hence we bring you the best testing facilities in a cost-effective way. We offer considerable discounts (15-20%) to our returning customers based on test volume and frequency.
    The turnaround time for astm d2116 test methodology depends upon the test procedure mentioned in the standard test document. However, we at MaTestLab understand your research requirements and hence try to get your test completed within the least possible time.
    Rohit Dhembare
    About Author
    Rohit Dhembare
    Rohit Dhembare is an Operations Associate at MaTestLab Inc. and holds a postgraduate degree in Organic Chemistry.
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