ASTM D5885 Standard Test Method for Low Strain Impact Integrity Testing of Deep Foundations

    What is ASTM D5885? 

    ASTM D5885 is a standard test method for measuring the oxidative induction time (OIT) of polyolefin geosynthetics using a high-pressure differential scanning calorimeter. The instrument records heat flow, and the time it takes to detect an exothermic oxidation reaction is the Oxidative Induction Time. The test method is to place a small specimen disc in an open aluminum pan in the pressure differential scanning calorimetry cell, pressurize the cell to a desired pressure with oxygen gas, and then increase the specimen temperature to a desired isothermal temperature. ASTM D5885 (Standard Test Method for Oxidative Induction Time of Polyolefin Geosynthetics by High-Pressure Differential Scanning Calorimetry) is applicable primarily to geomembranes and to geogrids, geonets, geotextiles, and other geosynthetics associated with polyolefins. Engineers use the measured OIT as an indicator of the antioxidant stabilization added to a geosynthetic product as received from a supplier, as part of quality control. 

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    Get Certified ASTM D5885 Testing for Reliable Geosynthetic Stabilization Performance 

    Certification verifies the conformance of a polyolefin geosynthetic to the ASTM D5885 specification, including OIT at set oxygen pressure and temperature. Before accepting a geomembrane or geosynthetic product for use in a landfill liner or containment system, or any other geosynthetic application, it undergoes an antioxidant stabilization test according to ASTM D5885 specifications. Testing and certification ensure compliance with ASTM D5885 criteria and reduce the risk of an early breakdown caused by oxidative degradation. 

    What is the Scope of ASTM D5885? 

    A high-pressure differential scanning calorimetry (DPSC) test is one of the standard methods used to determine the oxidative induction time of polyolefin geosynthetics. It is used to measure the durability of compounded polyolefins to oxidative degradation under high oxygen pressure at a controlled temperature. This standard provides a test method for determining antioxidant stabilization using a pressure differential scanning calorimeter (PDSC) under accelerated oxidative conditions. The primary purpose of ASTM D5885 is to determine the oxidative induction time of a polyolefin geosynthetic as a control method of antioxidant stabilization. 

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    The scope of ASTM D5885  includes:

    • Material type: Polyolefin geosynthetics such as geomembranes, geogrids, geonets, and geotextiles. 
    • Purpose: The purpose is to quantify for the evaluation of oxidative induction time and antioxidant stabilization. 
    • Properties evaluated: Oxidative induction time (OIT). 
    • Testing Method: Testing involves pressurizing a specimen disk in an oxygen-filled D.S.C. cell and heating to the isothermal test condition. 
    • Result: The oxidative induction time is reported in minutes at the specified test temperature and pressure. 
    • Test Limitations: he test standard is applicable to materials with an OIT > 30 minutes when tested at 3.4 MPa of oxygen at 150°C, and the results do not directly reflect the service life of a geomembrane. 
    • Use conditions: Oxygen pressure and isothermal test temperature significantly affect the measured oxidative induction time. 
    • Applications: Landfill liner and containment system quality control, geomembrane formulation comparison, geosynthetic supplier verification, antioxidant stabilization monitoring. 

    What are the Uses of ASTM D5885 Testing?

    ASTM D5885 testing is used to evaluate the antioxidant stabilization of polyolefin geosynthetic materials when exposed to accelerated oxidative conditions. Engineers use the results to compare formulations and to understand the oxidative resistance of a geosynthetic. This standard-

    • Assesses the oxidative induction time of polyolefin geosynthetics.
    • Enhances oxidative degradation artificially by increasing the pressure of oxygen.
    • Assesses antioxidant stabilization as received from a supplier.
    • Helps to compare the various geomembrane formulations at a given test temperature.
    • Aids in quality control monitoring of geosynthetic stabilization.
    • Assists in product development and formulation verification.
    • Helps in the selection of antioxidant packages for geosynthetic products.

    What Materials Can Be Tested Under ASTM D5885? 

    ASTM D5885 is used for polyolefin geosynthetics such as geomembranes, geogrids, geonets, and geotextiles, and is most commonly used for geomembranes. Common materials are geomembranes for landfill liners and polymembranes for containment applications, e.g., polyethylene, polypropylene. Analysts select a small specimen disc cut from the geosynthetic sample for testing. 

    Why is ASTM D5885 Important? 

    ASTM D5885 is a standard, accelerated method to determine the antioxidant stabilization added to a geosynthetic made from a polyolefin. Manufacturers and/or specifiers use this measured oxidative induction time as a quality control measurement, but the standard clarifies that the OIT value should not be used to predict the geomembrane’s actual service life. 

    ASTM D5885 Equipment and Sample Preparation Guide

    ASTM D5885 is a pressure differential scanning calorimeter-based method for measuring oxidative induction time at high oxygen pressure. Technicians select a small specimen disc from the geosynthetic sample for testing. The standard implements the test with increased oxygen pressure to speed up the test without significantly increasing the test temperature, which is dangerous for premature volatilization of the additive package. 

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    Sample and Specimen DetailsTechnicians use representative test specimens of polyolefin geosynthetics, including geomembranes, geogrids, geonets, or geotextiles 
    Specimen PreparationTechnicians prepare the test specimen according to standard procedures for high-pressure DSC analysis. 
    Specimen DimensionsSpecimen size depends on the DSC instrument requirements; the standard specifies appropriate specimen mass for the analysis. 
    InstrumentationTechnicians use a high-pressure differential scanning calorimeter (HP-DSC) capable of operating at 3.4 MPa oxygen pressure and 150 °C test temperature.

     Testing Procedures and Requirements for ASTM D5885  

    Technicians insert the specimen disc into the DSC cell and pressurize it with oxygen to the desired pressure, usually 3.4 MPa. The instrument then increases the temperature of the sample to a test temperature (typically 150°C), which is maintained at a constant temperature, and records the heat flux as oxidation proceeds as an exothermic reaction. 

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    Specimen Loading Technicians place the weighed specimen disc in an open aluminum pan and load it into the differential scanning calorimetry cell. 
    Oxygen Pressurization Technicians pressurize the cell with oxygen to the specified test pressure, typically 3.4 MPa. 
    Isothermal Heating The instrument heats the specimen to the specified isothermal test temperature, commonly 150°C, and holds it at that temperature. 
    Oxidation Onset Detection The instrument monitors heat flow and records the elapsed time until the specimen exhibits an exothermic oxidation reaction. 
    Data Analysis and Result Reporting Technicians determine the oxidative induction time from the DSC exotherm and then report the oxidative induction time (OIT) in minutes. 

    ASTM D5885 Testing Process and Data Collection

    Testing starts once the technician cuts and weighs a specimen disc from the polyolefin geosynthetic sample and puts it in an open aluminum pan. The technician then places the pan inside the differential scanning calorimetry cell and pressurizes the cell with oxygen to the desired test pressure. The instrument heats the specimen to the isothermal test temperature and maintains it at that temperature, measuring the heat flow continuously. The instrument senses the onset of an exothermic oxidation reaction and records the duration of the reaction. Finally, the analyst records this elapsed time as the oxidative induction time of the specimen under the given pressure and temperature conditions. 

     The image shows a polyolefin geomembrane specimen disc loaded into a pressure differential scanning calorimeter for oxidative induction time testing.
    ASTM D5885 High-Pressure Differential Scanning Calorimetry Testing of a Geomembrane Specimen

    Common Challenges and Troubleshooting

    The pressure inside the cell varies from time to time, which results in inconsistent oxygen pressure readings of the OIT, as the pressure directly affects the rate of oxidative acceleration. The measured induction time may also vary from one disk to another due to mass or thickness variation of the specimen unless these parameters are kept constant across the comparison. The isothermal hold period could cause a distortion of the onset detection of the exothermic reaction. Laboratories solve these problems by using a pressure calibration verification for the oxygen pressure, by preparing samples with uniform mass, and by maintaining uniform isothermal temperature control. 

    ASTM D5885 Analysis Results and Interpretation

    The report summarizes the results obtained from the measured oxidative induction time of the geosynthetic specimen of polyolefin. ASTM D5885 covers antioxidant stabilization behavior rather than a material overall performance rating.

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    • The laboratory measures the oxidative induction time in minutes under the specified oxygen pressure and isothermal temperature.
    • The technician will identify the type(s) of geosynthetic(s) being tested, whether that be geomembrane, geogrid, geonet, or geotextile.
    • The analyst notes the induction time obtained under the aforementioned pressure and temperature conditions and correlates the value with the antioxidant formulation of the tested material.
    • The engineer takes into account the test temperature, the oxygen pressure, and the type of resin when analyzing the results of oxidative induction time.
    • Engineers use the measured oxidative induction time values to support quality control and formulation comparison for polyolefin geosynthetics. 

    Link to ASTM D5885 

    FAQ

    What is oxidative induction time (OIT)?
    OIT is the time taken for a material to start oxidizing at an elevated temperature in high-pressure oxygen. It is a measure of the oxidative stability of the material.
    Elevated oxygen pressure speeds up the test and also permits a somewhat lower test temperature that produces a more accurate induction time measurement by preventing any volatilization or degradation of the antioxidant in the sample that would interfere with the measurement.
    OIT is one of the most important parameters of anti-oxidative resistance. In well-behaved systems, this test method is used as a quality control measure to monitor the stabilization in geosynthetics as received from a supplier.

    Updated on September 13, 2026

    Laraib Hashmi
    About Author
    Laraib Hashmi is an aspiring research enthusiast and science content professional with a strong interdisciplinary skill set, holding a postgraduate degree in Applied Microbiology from KIIT Bhubaneshwar, Odisha.
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