By Laraib Hashmi | Last updated 21st July 2026

ASTM D3166 Fatigue Properties of Adhesives in Shear by Tension Loading 

The ASTM D3166 test method specifies the preparation, loading, and testing parameters for measuring fatigue strength in shear by tension loading of adhesives on a standard specimen under specified conditions. The fatigue properties are a function of the specimen geometry.

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    What is ASTM D3166?

    ASTM D3166 is a standard method for evaluating the fatigue strength of adhesives in shear by tension loading, intended to define structural adhesives on a specific metallic substrate, using standardized specimens under specified conditions. While this test method is designed for metal-to-metal applications, it can also be used to measure the fatigue properties of adhesives with plastic adherends if the thickness of the plastic adherends is taken into account. ASTM D3166 (Standard Test Method for Fatigue Properties of Adhesives in Shear by Tension Loading (Metal/Metal) testing can be used to assess the fatigue performance of different adhesive systems or to compare them to the fatigue performance of joints created by other joining methods, utilizing simple joint geometries such as lap-shear or T-peel samples.

    ASTM D3166 Equipment and Sample Preparation Guide

    For ASTM D3166, the specimens are examined in an environment with a relative humidity of 50 ± 4% and a temperature of 23 ± 1.1 °C. The specimen is firmly gripped in the testing machine’s jaws. The cyclic load is applied in increments ranging from maximum to approximately 10% of maximum, and it is tested regularly.

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    Specimen Size

    For the ASTM D3166 test procedure, tension lap-shear specimens with precise dimensions and grip ends suitable for use in the particular testing equipment are used.

    What is the Testing Procedure and Requirements ASTM D3166?

    Each of the five specimens is subjected to five or more maximum loads, with failures occurring with regular spacing throughout a range of at least 10,000,000 to at least 2000 cycles. The number of cycles to failure, as well as the accompanying stresses in megapascals, are recorded. The measurements of the specimen bond are precise enough to calculate the area to the closest 0.6 mm.

    ASTM D3166 Result and Interpretation

    ASTM D3166 is a standard method for evaluating the fatigue strength of adhesives in shear by tension loading, to define structural adhesives on a specific metallic substrate, using standardized specimens under specified conditions. In accordance with ASTM D3166, the location of failure (adhesive or joint material) and nature of failure, if in the adhesive, are reported for each specimen.

    FAQ's

    Where can I get the astm d3166 tested?

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    How much do I need to pay for the astm d3166 test?

    Please contact us for a detailed quote for your astm d3166 testing needs. Cost incurred to carry out different astm d3166 testing methodology depends on the type of raw material; number of samples, coupons, or specimens; test conditions, turn around time etc. Costs of some ASTM testing methods start from $100 and the final value depends upon the factors listed above. Please contact us for the best and latest prices.

    How many samples are required for astm d3166?

    The required number of samples or specimens should comply with the procedure given in the astm d3166 standard. However, the MaTestLab operations team can assist you for your special requirements once you share your testing details with us.

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    MaTestLab has a vast testing laboratory network, hence we bring you the best testing facilities in a cost-effective way. We offer considerable discounts (15-20%) to our returning customers based on test volume and frequency.

    How many days will it take to complete the astm d3166 test?

    The turnaround time for astm d3166 test methodology depends upon the test procedure mentioned in the standard test document. However, we at MaTestLab understand your research requirements and hence try to get your test completed within the least possible time.

    Where can I get the astm d3166 tested?

    You can share your astm d3166 testing requirements with MaTestLab. MaTestLab has a vast network of material testing laboratories, spread across the USA and Canada. We support your all material testing needs ranging from specific astm d3166 test to various testing techniques.

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