| Specimen Preparation | Technicians prepare the required black glass panels, black-and-white hiding-power charts, and glass slides. They ensure that the substrates are suitable for the specified reflectance measurements. |
| Film Application | Technicians make manual drawdowns using a smooth, uniform motion at approximately 6 cm/s. They use a 150 mm-wide doctor-blade applicator with a clearance of 50, 75, 100, 125, 150, 175, or 200 µm, as required, and record the clearance used. |
| Film Drying | Technicians allow the trial drawdowns used for applicator selection to dry overnight before measuring their contrast ratios. For the subsequent test films, they follow the applicable drying and conditioning requirements of ASTM D2805. |
| Reflectance Measurement | Technicians measure the reflectance of each test area at a minimum of three locations, reading or estimating values to four decimal places and calculating the mean to the same precision. They place charts over a white surface and black glass panels over a black surface during measurements. |
| Spreading Rate Determination | Analysts calculate the experimental spreading rate, Hₓ, in square meters per liter (m²/L), using the template area, paint nonvolatile content, liquid density, and dry-film weight. |
| Density Determination | Analysts determine the liquid coating’s density in grams per milliliter (g/mL) per ASTM D1475. They use this value in the spreading-rate calculation. |
| Nonvolatile Content Determination | Analysts sandwich approximately 0.3 mL of paint between two previously weighed glass slides and squeeze it into a film approximately 45 mm in diameter. They weigh the slides with the paint, separate them, allow the films to dry, and weigh them again to determine the dry-film weight. They perform duplicate determinations and report the mean nonvolatile content as specified by the method. |
| Applicator Selection | Technicians make trial drawdowns on black-and-white charts using applicator clearances of 100, 150, and 200 µm. After allowing the films to dry overnight, they measure the contrast ratios and select an appropriate clearance to obtain a contrast ratio of 0.97 ± 0.01. |
| Drawdowns on Glass and Charts | Technicians use the selected applicator to prepare four drawdowns on black glass panels and four on black-and-white hiding-power charts. They retain sufficient uncoated white chart area to measure the substrate reflectance. |
| Calculation | Analysts calculate the coating reflectivity, R∞, from the chart measurements and determine the scattering coefficient, S, using the reflectivity, black-glass film reflectance, and experimental spreading-rate data. They calculate hiding power, H₀.₉₈, at a contrast ratio of 0.98. |
| Optional Contrast Ratio | When required, analysts calculate the contrast ratio, C, at a specified spreading rate, H꜀, using the calculated coating reflectivity and scattering coefficient. |
| Reporting | Analysts report hiding power, H₀.₉₈, reflectivity, R∞, scattering coefficient, S, and the applicator clearance. They also record the specified instrument information and other required worksheet results in accordance with ASTM D2805. |