ASTM C1351M Test Method for Measurement of Viscosity of Glass Between 104 Pa·s and 108 Pa·s by Viscous Compression of a Solid Right Cylinder [Metric]

    What is ASTM C1351M? 

    ASTM C1351M is the standard test method for measurement of viscosity of glass between 10⁴ pa·s and 10⁸ pa·s by viscous compression of a solid right cylinder (metric). It sets a standard laboratory method for measuring glass viscosity by observing deformation of a solid cylindrical specimen under a constant compressive force at a high temperature. This method is particularly useful for determining the viscosity-temperature relationship near the glass softening region and provides valuable information for glass-forming, thermal processing, research, and manufacturing process optimization.

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    Get Certified ASTM C1351M Glass Viscosity Testing

    The most significant property that determines glass forming, shaping, and thermal processing is glass viscosity. ASTM C1351M enables a reliable measurement of viscosity in the intermediate range where rotational viscometers are not always applicable, and beam bending methods are not yet applicable. The results help manufacturers to fine-tune production parameters and to develop materials with greater consistency and consistency in their development.

     The image shows a high-temperature compression viscometer measuring the viscosity of glass using solid cylindrical specimens under compressive loading as per ASTM C1351M.
    ASTM C1351M High-Temperature Compression Viscometer

    What is the scope of the ASTM C1351M standard test? 

    ASTM C1351M provides a standard test method for determining the viscosity of glass using viscous compression of a small solid cylindrical specimen. The test method-

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    • Determines the viscosity of glass by viscous compression.
    • Measures viscosity between 10⁴ Pa·s and 10⁸ Pa·s. 
    • Uses a solid right cylindrical glass specimen.
    • Applies continuous compression under high temperature. 
    • Assists in the determination of the viscosity-temperature relationship. 
    • Supports glass production, research, and quality control applications.
    • Gives viscosity values in standard metric units.

    What are the Uses of ASTM C1351M Testing? 

    ASTM C1351M determines the viscosity of glass within the range of approximately 10⁴ Pa·s to 10⁸ Pa·s by measuring the deformation rate of a solid cylindrical specimen under a constant compressive load. The test supports manufacturers in optimizing glass-forming processes, thermal behavior evaluation, and consistent product quality.

    • Measures the viscosity of glass by analyzing viscous compression behavior.
    • Evaluates the flow behavior of glass at elevated temperatures.
    • Helps optimize glass forming and shaping processes 
    • Assists in material development and product qualification. 
    • Verifies viscosity-temperature relationships. 
    • Compares properties of various glass types in terms of their processing. 
    • Assists with quality control and manufacturing consistency.

    Which materials can be tested under ASTM C1351M? 

    Glass materials with viscosity ranging from about 10⁴ Pa·s to 10⁸ Pa·s are within the scope of ASTM C1351M. The laboratories use this method for commercial, specialty, laboratory, and engineering glasses within the intermediate viscosity range.

    Why is ASTM C1351M Important? 

    ASTM C1351M is a standard method for measuring glass viscosity within an intermediate range. This helps manufacturers fine-tune their forming process, boost productivity, and ensure consistent thermal processing characteristics.

    Common Challenges and Troubleshooting 

    Accurate viscosity measurements require precisely machined cylindrical specimens, uniform furnace temperatures, constant compressive loading, and accurate deformation measurements. Common problems are dimensional inaccuracies in specimens, non-uniform loading surfaces, temperature fluctuations, instrument calibration errors, misalignment during compression, and variable deformation measurements. Proper specimen preparation, equipment calibration, and controlled testing conditions produce accurate and reliable results.

    ASTM C1351M Testing Process and Data Collection Guide 

    Technicians begin testing by preparing a representative solid cylindrical glass specimen according to the dimensions specified in ASTM C1351M. The technicians place the specimen between compression platens inside a high-temperature furnace and heat it at the required temperature. The technician then subjects the specimen to a constant compressive load and continuously measures the resulting decrease in specimen height. At the time of testing, the laboratories document the specimen size, load, temperature, rate of deformation, duration, and displacement. Engineers use these measurements to determine the viscosity of the glass for the given temperature range.

    ASTM C1351M Equipment and Sample Preparation Guide 

    The viscosity measurements require careful preparation of the cylindrical glass specimen; the furnace temperature has to be steady; the specimen has to be subjected to a steady compressive loading, and the deformation has to be carefully measured. For reliable and repeatable viscosity data, proper specimen geometry is needed, along with smooth parallel loading surfaces and calibrated instrumentation.

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    Sample and Specimen DetailsTechnicians prepare representative solid cylindrical glass specimens from the test material for viscosity measurement.
    Specimen PreparationPrepare solid cylindrical specimens with parallel, smooth end faces; check size and look for defects before testing.
    Specimen DimensionsThe technician prepares and accurately measures the diameter and height of the cylindrical specimen because these dimensions are required for viscosity calculations.
    InstrumentationHigh-Temperature Compression Viscometer, High-Temperature Furnace, Compression Loading System, Load Cell, Linear Displacement Measuring Device (LVDT), Thermocouples, Temperature Controller, Data Acquisition System.

    Testing procedures and requirements for ASTM C1351M

    ASTM C1351M is a standardized viscous compression technique for viscosity measurement of glass. The reliability and repeatability of a viscosity value from the furnace is obtained by ensuring accurate preparation of the specimen, accurate furnace temperature control, constant compressive loading, and accurate deformation measurement.

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    Solid Cylinder Specimen Preparation Technicians prepare a representative solid cylindrical glass specimen with smooth, parallel end surfaces according to ASTM C1351M.
    Controlled Heating and Compression (CHC)The technician places the specimen in the high-temperature test system, heats it to the required temperature, and applies a constant compressive load.
    Compression Deformation MeasurementTechnicians continuously measure the change in specimen height as viscous deformation occurs during the test.
    Viscosity CalculationCalculate the glass viscosity based on the measured deformation rate, specimen dimensions, applied load, and test temperature.

    Analysis Results and Interpretation 

    • The ASTM C1351M method measures the viscosity of glass by measuring its deformation when subjected to compressive loading. 
    • Viscosity is normally reported as pascal-seconds (Pa·s) in laboratories along with the test temperature, compressive displacement, and deformation rate in the test (mm/s or mm/min).
    • Other testing parameters, which are necessary for viscosity calculations per ASTM C1351M, are also reported by the testing laboratory, such as specimen dimensions, applied load, test duration, and calculated deformation rate.
    • Manufacturers use these values to compare the processing characteristics of the glass and to determine the optimal manufacturing conditions.

    Link to ASTM C1351M

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    FAQ

    Where can I get the astm c1351m tested?
    You can share your astm c1351m testing requirements with MaTestLab. MaTestLab has a vast network of material testing laboratories, spread across the USA and Canada. We support your all material testing needs ranging from specific astm c1351m test to various testing techniques.
    Please contact us for a detailed quote for your astm c1351m testing needs. Cost incurred to carry out different astm c1351m testing methodology depends on the type of raw material; number of samples, coupons, or specimens; test conditions, turn around time etc. Costs of some ASTM testing methods start from $100 and the final value depends upon the factors listed above. Please contact us for the best and latest prices.
    The required number of samples or specimens should comply with the procedure given in the astm c1351m standard. However, the MaTestLab operations team can assist you for your special requirements once you share your testing details with us.
    MaTestLab has a vast testing laboratory network, hence we bring you the best testing facilities in a cost-effective way. We offer considerable discounts (15-20%) to our returning customers based on test volume and frequency.
    The turnaround time for astm c1351m test methodology depends upon the test procedure mentioned in the standard test document. However, we at MaTestLab understand your research requirements and hence try to get your test completed within the least possible time.
    Gokula Srinivasan Selvam
    About Author
    Gokula Srinivasan Selvam
    Gokula Srinivasan Selvam is a Material Testing Associate at MaTestLab Inc. and holds a postgraduate degree in Ceramic Engineering from IIT (BHU), Varanasi.
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