By content81c70d6e36 | Last updated 9th March 2026

ASTM B963 Standard Test Methods for Oil Content, Oil-Impregnation Efficiency, and Interconnected Porosity of Sintered Powder Metallurgy (PM) Products

ASTM B963 provides a standardized procedure for determining the oil content, oil-impregnation efficiency, and interrelated porosity of sintered powder metallurgy (PM) products. It employs the Principle of Archimedes in calculating volume and oil immersion methods in the study of the amount of oil that an object can absorb and hold. The tests play a critical role in self-lubricating PM bearings and other similar materials, guaranteeing good performance, quality, and durability.

Read More

GET STARTED

    Share your requirements *

    Provide your contact information *

    Introduction to ASTM B963

    Powder metallurgy (PM) products are popular in self-lubricating applications, including bearings, bushings, and other mechanical components. Their performance is mainly determined by the porosity of the material and the storage and release of oil in the process of operation. ASTM B963 uses standardized test methods to assess these critical properties with emphasis on the following three aspects: the oil content of a specimen, which determines the lubrication capacity of a specimen; the efficiency of oil-impregnation, which is the ability of pores to fill during manufacturing; and the interconnected porosity, which is the network of pores in which the oil can be held.

    Get Certified ASTM B963 for Accurate Evaluation of PM Porosity and Lubrication

    ASTM B963 certification assures that the sintered PM products are evaluated under standardized tests that measure the level of oil content, efficiency of impregnation, and interconnected porosity. Certified testing gives reliable data on quality control, process optimization, and the reliability of the product.

    Service NameRemarks
    ASTM B963 Testing
    Contact US

    ASTM B963 Testing Procedure and Requirements

    EquipmentASTM B963 needs a very accurate analytical balance, checked with a standard mass. The impregnation of the specimen is done in an oil bath or a vacuum setup, and measurements by Archimedes require the use of a water immersion setup
    Sample PreparationThe maximum mass per specimen should be 1.0 g. In smaller sizes, several of them can be compounded. Weighing should be done at a uniform temperature of the specimen, the balance, and the surroundings.

    Scope of ASTM B963

    • Test oil content, impregnation efficiency, and related porosity of sintered PM products.
    • Can be applied to self-lubricating bearings, bushings, and porous structural components.
    • Defines impregnation, extraction, and mass measurement procedures.
    •  Helps to assess pore interconnectivity and lubrication efficiency.

    ASTM B963 Equipment and Sample Preparation

    Specimen PreparationSintered PM specimens are cleaned, dried, and weighed; samples are then impregnated with oil under vacuum or pressure to fill interconnected pores before testing.
    Specimen SizeRepresentative PM components such as bearings, bushings, or machined test samples are selected for evaluation.
    Specimen DimensionsDimensions are measured to assist in density and porosity calculations, though mass-based measurements primarily determine oil content and impregnation efficiency.

    Applications of ASTM B963

    • Bushing and sleeves of powder metallurgy powder.
    • Engine and transmission components of the auto PM.
    •  Porous structural components of industrial machinery.
    • Aerospace PM lubrication of important parts.

    ASTM B963 Common Challenges and Troubleshooting

    The correct testing requires the consistency of the temperature of weighing. It can be variable in case the specimen being used is too small or irregularly surfaced or when the oil is not impregnated. Moreover, the balance of analysis will need to be calibrated appropriately, and the results will need to be replicated to ensure feasibility.

    ASTM B963 Aggregate Testing Technique, Process, and Data Collection

    The specimen is dried and put on a scale until it attains its initial mass is obtained. This is followed by an oil impregnation process, which is usually under vacuum or pressure to guarantee oil filling of interconnected pores. The specimen is then weighed after impregnation to find out that the oil has been uptaken. Oil recovery can be done to analyze the oil retained and the porosity feature. Oil content, impregnation efficiency, and interrelated porosity are computed based on mass differentiations and density values. All outcomes are documented for comparison with the given product performance specifications.

    ASTM B963 Analysis Results and Interpretation

    Acknowledged performances show that the PM material has enough interlocking porosity to hold lubricant and help it to perform as a self-lubricant. The increased oil content and effective impregnation imply good pore connectivity and high operational durability. Low retention of oil or variable porosity measure could be a measure of poor sintering, closed pore structure, or lack of proper impregnation measures.

    ASTM B963 Problem & Solution

    Unless the interconnected porosity and efficiency of impregnation with oil are controlled or reviewed. ASTM B963 provides standardized test methods to quantify oil content, impregnation efficiency, and interconnected porosity.

    Factors to Consider for ASTM B963

    Speed
    To enable efficiency in the testing productivity, efficient impregnation, extraction, and weighing processes are essential to retain the accuracy of measurement.

    Expert
    The technicians must be experienced in handling the vacuum impregnation processes, accurate in mass measurements, and capable of proper calculation of the parameters of porosity and retention of oil during processing.

    Cost
    ASTM B963-compliant standards enhance the consistency in lubrication, minimise failures caused by wear, and lower the cost of maintenance in the long term of the PM components. 

    FAQ's

    Where can I get the astm b963 tested?

    You can share your astm b963 testing requirements with MaTestLab. MaTestLab has a vast network of material testing laboratories, spread across the USA and Canada. We support your all material testing needs ranging from specific astm b963 test to various testing techniques.

    How much do I need to pay for the astm b963 test?

    Please contact us for a detailed quote for your astm b963 testing needs. Cost incurred to carry out different astm b963 testing methodology depends on the type of raw material; number of samples, coupons, or specimens; test conditions, turn around time etc. Costs of some ASTM testing methods start from $100 and the final value depends upon the factors listed above. Please contact us for the best and latest prices.

    How many samples are required for astm b963?

    The required number of samples or specimens should comply with the procedure given in the astm b963 standard. However, the MaTestLab operations team can assist you for your special requirements once you share your testing details with us.

    How much discount can I get on the astm b963 test?

    MaTestLab has a vast testing laboratory network, hence we bring you the best testing facilities in a cost-effective way. We offer considerable discounts (15-20%) to our returning customers based on test volume and frequency.

    How many days will it take to complete the astm b963 test?

    The turnaround time for astm b963 test methodology depends upon the test procedure mentioned in the standard test document. However, we at MaTestLab understand your research requirements and hence try to get your test completed within the least possible time.

    Where can I get the astm b963 tested?

    You can share your astm b963 testing requirements with MaTestLab. MaTestLab has a vast network of material testing laboratories, spread across the USA and Canada. We support your all material testing needs ranging from specific astm b963 test to various testing techniques.

    POPULAR TESTS
    ONE-STOP FOR ALL
    MATERIAL TESTING NEEDS
    MaTestLab Inc. offers accessible, quick, and affordable material testing, product testing, and failure analysis services. We support your on-demand testing and expert consultation needs with the help of our extensive network of material testing laboratories situated in the US and other parts of the world.
    MATERIAL TESTING
    We offer destructive and non-destructive tests over a range of mechanical, electrical, chemical, thermal, optical, corrosion, radiation, and biological testing methodologies defined by ASTM, ISO and other organizations.
    PRODUCT TESTING
    We help you evaluate and ensure your product quality and performance with standard and custom-made testing solutions. All the tests are done at well-equipped testing laboratories using standard testing methods for best output and satisfaction.
    FAILURE ANALYSIS
    Failure analysis ensures high levels of quality in every manufacturing process. We help you with getting the best failure or root cause analysis to determine the cause of the failure. The results help you identify means to prevent failure recurrences.
    Process for testing
    • STEP 01

      You share your testing requirements

    • STEP 02

      You share your sample(s)

    • STEP 03

      We deliver your test reports

    Get your testing done

    Let us known your testing requirements and we will be right back with a solution.

      Let us root for each other. Collaborate to grow, expand, and accelerate our businesses.

      Partner with us

        close

        Please share your requirement with us

          ×

          Contact Us

          Discover more from MaTestLab

          Subscribe now to keep reading and get access to the full archive.

          Continue reading